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Papers of the Stepney family of Prendergast, Pembrokeshire, and Llanelli, Carmarthenshire, mainly deeds relating to their estates in those counties, 1541-1787, including deeds concerning the working of coal in the Llanelli area of Carmarthenshire in the 17th-18th centuries; and family and business letters, 1706-1829, of the Stepney family including letters relating to the trading enterprises of Sir Thomas Stepney, seventh baronet, 1749-1767, which include letters from the masters of his ships, from other business firms, and from his agents in the main seaports of Wales and England as well as at continental centres of trade, such as Brest and Lisbon. Despite its title, there are no papers relating to the Cilymaenllwyd estate.

Records, 1701-1910, of the business concerns of Charles Nevill, his son, Richard Janion Nevill and Nevill, Druce and Co., notably the Swansea Copper Works and the Llanelli Copper Works and collieries in Carmarthenshire, 1797-1910, including: a diary of Charles Nevill containing entries relating to the Swansea Copper Works and to analyses of copper ore, 1797-1802; copies of letters written from Llanelli, 1812-1813, and diary entries relating to lead works, 1811-1813, and to roadmaking at Llangennech, 1812-1813; letter books, 1804-1832; colliery accounts and reports, 1803-1836; bye-laws of the Llanelli Copper Works, 1805-1834; accounts of the sale of copper, rough copper books, etc., 1807-1874; ticketings of lead mainly from mines in Cornwall, Cardiganshire and the Isle of Man, 1852-1853; entry books of offers of lead ore, 1851-1876; registers of purchases, 1860-1875; lead ore produce books, 1862-1872; an account book of the steamer Harriet, 1838-1840; shipbuilding specifications, 1865-1872; and a large number of deeds and documents, 1701-1910, including industrial leases in Llanelli. Papers of Charles William Nevill are not included.